1/9/97


Dear All

I would appreciate suggestions for examining 80 micron

eggs in seawater or distilled water by SEM where the user

wants to compare fresh egg surfaces (therefore cryo?) with

conventionally fixed, dehydrated and critically point dried

eggs.

The idea was to use cryoSEM but there are problems. I

have tried freezing (in ethane) on a thin smear of Tissue Tek

OCT - droplet on stub and then wiped off with cover slip (not

easy in itself?), but the eggs sank, never to be seen again!

I have also frozen them just mounted in a water film, but

some have simply sheared off the standard smooth stub -

should I try poly-L-lysine or super glue?

A separate problem seems to be that while the crustacean

in question is marine/estuarine and the eggs stand fresh

water for a while (therefore for rinsing), even after 3 or 4

distilled water changes I still see a fine, dried layer of

salt over everything. The rinsing is done in a watchglass

and the water was almost completely removed with an

autopipette before refilling.

One idea not tried yet is to place an egg on a millipore filter,

drain on filter paper, place on stub in cryoSEM airlock

cold-stage and freeze in situ. But with or without vacuum?

It seems a crazy world when it is easier to ask internet

friends than it is to search through a bucket a mud and then

do the experiments on the method to use!

Any comments would be appreciated. Take up gardening?

Thanks in advance - Keith Ryan

Plymouth Marine Laboratory, Citadel Hill,

Plymouth, Devon PL1 2PB, England

e-mail: k.ryan@pml.ac.uk

PML web site: http://www.npm.ac.uk/pml


Kieth,

To look at surfaces of small samples, roughening the stub surface

with fine sandpaper will help keep the ice on the stub during cryo, but we

went into overkill and machined a slight "well" in the surface of the stub

and then roughed it up. To get a cross sectional view, we drill several

small wells (1/16 in.dia x 1/8 in. deep) in the stub. Overfill the wells

(this can be tricky) with a high concentraion of sample in water leaving a

slight droplet (protruding meniscus) of sample protruding above the well.

Sometimes a little vaseline on the surface will help keep the droplets from

running together. Freeze and shear off the droplets.

For the dry eggs, we would use about a dozen (pelco #16079)

adhesive tabs stuck on the surface of a clean glass slide. Dissolve these

into 20 ml chloroform. Place a drop or two of this solution on the surface

of the stub (or coverslip for a smoother background surface), spread evenly

and drain the excess with the corner of a kimwipe. This usually produces a

very thin layer of adhesive strong enough for samples up to a few hundred

microns.

As for the salt on the surface after 3 or 4 washes, not much help

I'm afraid, just a thought. Is there a mucosal surface layer that the

distilled water is drawing the salt out of ?? If so, they might need an

EDTA treatment first to remove mucus. Then again, this mucus might be the

surface you need to see??? This might be a case of "a rock and a hard

place", but sucessful cryo should tell you what is on the surface if you

can get a fracture through an egg.

Hope this is helpful.

Cheers

:)

George

Department of Earth and Atmospheric Sciences

University of Alberta

Edmonton, Alberta T6G 2E3

Canada

ph: 403-492-5746

fax: 403-492-2030

george.braybrook@ualberta.ca


Keith,

One way to examine your marine eggs would be to use the high-pressure

freezer to freeze a suspension of washed eggs in distilled water (a roughly

200 micrometer thick plug, 1000 or more micrometers in diameter). Then

fracture, etch, and coat as for a TEM replica but use the cryoSEM to look

at the rough surface of the fracture. By regulating the amount of etch you

could see the surface of the egg as well as cross-sections of the layers of

the walls. Paul Walther's articles on double layer coating may be

helpful.

Jacob

Jacob Bastacky, M.D.

Room 116 Donner Laboratory

Lawrence Berkeley Laboratory EMail: sjbastacky@lbl.gov

University of California Phone: (510) 486-4606

Berkeley, California 94720 Fax: (510) 486-4750


Keith,

Excellent cryo-fracture images of single cells can also be produced,

using the Tissue-Tek/Carbon mixture. (My earlier note) It is also a good

adhesive, especially on the rough cryo-stub surface. George had very

good ideas on cryo-stub surface preparation.

This mixture also fractures well, exposing ALL inner surface of the

fractured eggs "embedded" in it. I hope it will work well for you.

Regard,

Laszlo

Laszlo J. Veto

Electron Microscopy & Image Analysis

Pacific Agri-Food Research Centre, AAFC

Ph: 250-494-7711

e-Mail: vetol@em.agr.ca


Keith,

My recommendation would be to use a mixture of Tissue-Tek and carbon

dust (from carbon rod sharpener) paste on your cryo-stub. In this

mixture the eggs will not sink fast, therefore will have time to carry out

the freezing process.

I have great LTSEM results using this mixture with unfixed single cell

culture and bacteria.

The separate problem about the fine layer of salt, (if the osmatic change

is all right!) use larger amount of distilled water to rinse for longer time.

Good luck,

Laszlo J. Veto

Electron Microscopy and Image Analysis

Pacific Agri-Food Research Centre

AAFC

vetol@em.agr.ca


Hi Keith,

It occurred to me that to be sure that your treatments did not introduce any

artefacts on the egg surface you might try a Wild (Leica) Elsam accoustic

microscope. I'm not very familiar with them but there is the potential (at

least) to look at them in seawater or other isotonic solution.

Just a thought,

Geoff Avern

Australian Museum

geoffa@amsg.austmus.gov.au


Keith,

Here is my 2 cents.

1. Coating of poly-L-lysine do help the sample adhere to substrate.

2. Did you have tried freeze-substitution followed by either fast-freezing

again, freeze-drying, cryo-coating, and cryo-SEM observation, or

dehydration, critical point drying, and SEM observation at RT?

3. I agree with George Braybrook's comment that there is a mucous layer on

the egg surface.

With best wishes!

Ya Chen

My email address has been changed to: ychen14@facstaff.wisc.edu ***

Integrated Microscopy Resource (IMR)--

an NIH Biomedical Research Resource TEL : 608-263-8481

University of Wisconsin-Madison FAX : 608-265-4076

1675 Observatory Drive #159 Email1:ychen14@facstaff.wisc.edu

Madison, WI 53706 Email2:chen@calshp.cals.wisc.edu


You have two major problems:

Sticking and retaining the processed eggs onto a substrate prior to coating and

earlier, removing all traces of salt from the eggs

.

You could try poly-l-lysine. The old technique, which works well for

specimens of that size range, is a drop of a sticky solution onto a

substrate. After solvent evaporation a very thin "permanently" sticky layer

remains.

The solution is prepared by dissolving the gum of clear sticky tape

in chloroform overnight. Push a couple of meters of tape into a small jar

and add about 50 ml of chloroform. If you require a very clean background

the solution can be millipore filtered.

If some low power images are needed, than freshly cleaved mica gives

a very clean background. At zero tilt, the mica is very dark in secondary mode.

Removing salt from marine specimens can be very difficult. Leaving

the specimen for a lengthy period in water, even after fixation, may damage

structures. An appropriate concentration of ammonium acetate provides the

right molarity and the aqueous (or ethanol) solution leaves no residue.

Others have referred to mucous which may or may not be removed. EDTA

fell out of favour as a decalcifier some time ago. For the same reasons I

would prefer a broad spectrum enzyme. I used a snail enzyme many years ago

for removing mucous, but your local biochemist should be able to advise.

Hope this is some help with this difficult problem.

Happy New Year

Jim Darley

Probing & Structure (Microscopy Supplies & Accessories)

PO Box 111, Thuringowa QLD 4817 Australia

Phone +61 77 740 370 Fax: +61 77 892 313

A great microscopy site: http://www.ultra.net.au/~pns/

p&s@ultra.net.au


Keith and fellow microscopists,

Tony King of VG Microtech in the UK (who produce a cryo-SEM, the Polaron

LT7400) had some additional comments which he asked me to pass along:

>> >My recommendation would be to use a mixture of Tissue-Tek and carbon

>> >dust (from carbon rod sharpener) paste on your cryo-stub. In this

>> >mixture the eggs will not sink fast, therefore will have time to carry out

>> >the freezing process.

Tony replies:

Try tissue tek smear (with carbon dust on a Dry colloidal graphite base;

this absorbs the tissue tek bulk and holds the samples in place.

>> >I have great LTSEM results using this mixture with unfixed single cell

>> >culture and bacteria. The separate problem about the fine layer of

salt, >> >(if the osmatic change is all right!) use larger amount of

distilled water >> >to rinse for longer time.

Tony replies:

>Use Osmium vapour to semi-fix the cells before plunging into water.

>Osmotic shock is then reduced to minimum.

>Regards,

>

>Tony King

>Product specialist

>VG Microtech/ Polaron range

>

>Tel: +44 (0)1825 746251

>Fax: +44 (0)1825 768343

>

>E&OE

>

Best regards,

steven E. Slap

Energy Beam Sciences, Inc.

Adding Brilliance To Your Vision

ebs@ebsciences.com

http://www.ebsciences.com/


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